Shopping list 4mmc / 3cmc synthesis

[1019er]

So imm getting further im buying chemicals for my first synthesis.

As I have seen producing 3cmc seams as easy as 4mmc (the easy method)

So my ingredients will be:

2B4M - 100 g
DCM - 300 ml (Toluene)
Xylol
Methylamine 40% aq solution - 200 ml
Hydrochloric acid - 50 ml
Dry acetone - 200 ml

Now I only need to order toluene via Amazon .
And then I need a good nearby supply for methylamine and 2b4m.

With the lab equipment im ready to go to produce my first batch of mephedron!

For 3mmc it seems that I only need:
to synthesize this substance so I think it's a good idea to produce this as well if there's a demand.

So my ingredients should be:

2B2C - 100 g
DCM - 300 ml (Toluene)
Methylamine 40% aq solution - 200 ml
Hydrochloric acid - 50 ml
Dry acetone - 200 ml

I will keep you updated when im closer to synthesis!

 

[gus.fring]

Waiting for your resault

 

[The-Hive]

@Berlin777 check this out…

 

[Berlin777]

its 3mmc, I am trying 3cmc. Acetone HCl not worked well. Already had some result with aqueous crystallization but low purity. I'll see how the rest of samples gonna turn out. But thanks anyway.

 

[fosties]

Just to give you a little update.

I still have to buy the Destillation kit, the vacuum pump I already bought lately I'm still looking for the toluene and a good source for 2B4m to get my hands on.

 

[momogf]

Made 2b4m your self then u get him cheap

 

[fosties]

I found a source for Toluol and xylol and HCL Acid (37%) and 100% Aceton (from Amazon I will have dry it)

I didn't found out how much % the HCL acid should have?



Now I need:


2B4m - maybe I'll produce it bymself if I can get the all the substances to synthesize it.
Please tell me a easy method!

Methylamine - don't know where to get it. Please tell me!!


When it comes to technical equipment, I already got a vacuum pump+chamber, Buchner filter and a few measuring cups, spoons, a fine scale etc.
I also own a mask+filter, full body safety suit.

My next investment will be lab equipment to finish my setup also for further projects.

Vevor 2000ml Lab heater 220 V.
Or can I also buy the cheaper 1000ml?

Vevor 1000 Destillation kit 32 parts

2x Lab stand, lab glass etc.

2000ml flasks for the heater.
If necessary?



Wouldn't be nice if anybody has tips for my lab setup.

I'm not sure if it's necessary to invest a few 100€ more in 2000ml flasks+heater etc. I only produce for myself.

My plan is to learn how to produce different substances as a hobby and out of an long lasting interest in different substances and how they are made.
So everything should not be too expensive, because I will not have a financial return of this project!!!

If anybody is or was in the same situation and is willing to guide me into the right direction, I would be super thankful!!!