4MMC/MEC large crystals

Sergey Kush

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4-mmc in water.
 

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infochem

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Hi, only water? Please tell me proportion ,temperature and time.
 

Heineken

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My new way made crystal now they are *****ing hard and is very hard crash with credit card and they are real big :)
Now they are grow is 1 day
 

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Heineken

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For today nice ice pure crystal.
need dry 1h and this all ready to use:)
 

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antrax

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what´s the point of crystals and not leave it in the hydrochloride form? I don't think a crystal can be snorted.
can you explain it to me, thank you!!
 
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xile

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Are you on the right webside? Of cours the crystals where grindet and snorted or crystals where eaten.
 

Goku

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on first time made is no so bad :)
 

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Goku

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To prove that a miracle can be done.($)
 

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Albert A

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Dear friends, does anyone know how to make such a beautiful crystal (stone) from 4-mmc ?
 

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Gordon Ramsay

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Looks like cocaine to me :D
 

Albert A

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4mmc was made into a form very similar to cocaine.
That's the whole point.
 

Gordon Ramsay

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Very interesting :) Well I would say it is perfectly purified powder pressed like they do it with cocaine I think
 

Eureka

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Here’s a photo of 4MMC in water heated to saturation at 95deg in a pot, then placed in an insulated cooler with boiling water added as a bath.

The cooler is closed and covered with a sleeping bag. Opened after 24hrs.

As long as the solution is clean the result is 0.8-1.2cm width crystals.
W01M64hd35
 
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The gradual cooling method works the same way as all the others. The solubility of 4mmc at a lower temperature drops and the crystal begins to grow. The slower the temperature changes, the larger the crystal grows.
One disadvantage is that even after crystallization is complete, some 4mmc remains in the water. Therefore, it is better to use two solvents.
 

Acidosis

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A large percentage of water and a lower percentage of solvent will create perfect crystals and the solvent will retain and save the rest of the product for later extraction.
RugKdlCsiI
 

HerrHaber

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X-ray diffraction pattern would make this more convincing (haven't seen such 4MMC since 2010, therefore I know they can be as such but I never personally obtained them). P.S. I haven't got any actual competence in interpreting XRD data...
 

Gordon Ramsay

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Acidified into the aeq. layer, cleaned the aeq. layer with DCM and crystallized with 2:1 Water:Acetone solution 🐱 💎

OxBLdSpQ40
 
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