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what ratio?

If I have amphetamine freebase in toluene how do I precipitate amphetamine sulfate, do I dilute sulfuric acid with acetone or isopropyl alcohol?

https://epdfx.com

https://www.scribd.com/document/329301415/Conversion-of-APAAN-%CE%B1-phenylacetoacetonitrile-into-BMK-benzylmethylketone

I am interested in conducting a synthesis of Phenylacetoacetonitrile under phase transfer conditions using aliquat 336(15grams per mol of phenylacetonitrile) and 50% sodium hydroxide solution(as water or (methanol 60grams in 200ml)/ polar phase) with toluene as non polar phase, ethyl acetate as...

Can the acetic acid be replaced with formic acid?

Can anybody tell me how important to the reaction proceeding is the presence of water in the reaction mixture?

If I add the reaction mixture and no reaction begins, I must heat it to start it yes?

Cam somebody in great detail describe to me the exact moment I should pour off the mercuric solution from the aluminum when preparing an aluminum amalgam? It is unclear if there needs to be a heavy gray thick precipitate or not.

I wouldn't do anything I couldn't scale up, in for a penny in for a pound.

There are two methods by which I can reduce nitrostyrene to amine, 1 is a procedure authored by sunlight here; https://www.erowid.org/archive/rhodium/chemistry/nitrostyrene.reduction.alhg.html, the second method is detailed here and used to the synthesis of amphetamine...

This is *****ish, time is most valuable, you need to start as close as possible to finished product, or produce something with chemicals that are easier to get, reducing nitrate is a waste of time.

don't worry I found the source https://www.erowid.org/archive/rhodium/chemistry/anhydrides.html

Can you provide me a source for this;

G patton can you provide a source for the procedure wherein sulfur monochloride is produced in situ, if sulfur dioxide is emitted so as to complete the reaction I don't see how sulfur can be catalytic, unless acetyl chloride is being generated.

If you can obtain anhydrous sodium acetate, then via dry distillation with sodium bisulfate glacial acetic acid is distilled off.

Can you post a link to the source of this information, and what is the purpose of the activated carbon step? Is this personal experience?

should I use a 1:1 molar amount of base to adduct?

Can you be more specific? What should the concentration of the solution be?, how much volume of solution should I use for say 30 grams of adduct , does it matter?

Can you described to me exactly how to purify by bisulfite adduct.