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Because I haven't crystallized it yet.

90ml nitroethane,90ml benzaldehyde,70ml GAA and 70g ammonium acetate. The details were previously written above.

Ammonium acetate is the best option if you cannot obtain cyclohexylamine. The yield is not bad and the product is not very dirty. It only needs to be recrystallized once. The last time I did the synthesis the yield was 100g from 90ml Nitroethane. I haven't recrystallized it yet

I think that the common way to grow khat is by cuttings. It is also possible to grow khat by seeds, but it is not common.

This is my experience with ammonium acetate: 80ml benzaldehyde 80ml nitroethane 60g anhydrous ammonium acetate 70ml GAA refluxed In a water bath, the temperature is close to boiling (I think 90°-95°) for 5-6h. Shake the flask periodically After 6h: Let it cool to room temperature and...

Thanks I will look for that. And if I can't be patient, I'll try the other option

There was a little oil floating on top of the water And there was a benzaldehyde smell This picture after heating for four hours Then separate the aqueous layer, pour IPA and Put it in the freezer for 10 hours And this is after shaking No crystals appeared, then I evaporated I PA...

I put 10ml benzaldehyde, 10ml nitroethane, 2.5ml GAA, and 4g ammonium acetate in a flask Heating at 60-70 °C for 4 hours. After cooling to room temperature, there were two layers, at the bottom a yellow layer and at the top a white layer. I put it in an ice bath for 2 hours (I don't have access...

I've seen a video about this synthesis before, but it was in Russian If you are interested let me know and I will look for it

I haven't used it before but I think this video will help youthis video

How much ammonium acetate and GAA do I need to add to 10g benzaldehyde and 10g nitroethane thanks in advance

Synthesis of APAAN (a-phenylacetoacetonitrile) with sodium amide (1kg scale)

Can you tell me all the steps of synthesis with ammonium acetate How many ml of ammonium acetate did you use? Did you use acetic acid? Reflux time? yield? Thanks in advance

Thank you. I have also read this method in previous replies. And Someone in the replies said: The thing that I understood is that if I add acetic acid, I will not need a high temperature, and the synthesis time will decrease. If I did the same amount as in the thread said 100ml...

It is not available locally, and if you order it online, it will take more than a month to get here. ammonium acetate i can get it today

I can't get cyclohexylamine nor butylamine but I can get ammonium acetate. I'm going to do 100ml benzaldehyde, 100ml nitroethane and 25ml acetic acid. So how much ammonium acetate will I need?

If you want it for personal use, it should not be in the form of a pill Just weigh the powder and you will know how much the pill weighs. But if you want to make pills for resale or any other reason, you will need a pill die (you can buy it from AliExpress). Weigh the powder and put it in...

Where I live there is no limit to buy pseudoephedrine pills so I can buy any quantity

I haven't tried it. Ask the experts. They may have knowledge and advice @G.Patton @HIGGS BOSSON

I found this