Search results

  1. Mohammed_Lee

    Suction (vacuum) filtration

    It's pretty easy to built your own "vacuum desiccator" if you got a vacuum source. I just drilled a hole in a pot for the vacuum hose and sealed the cap. Works fine for small scale.
  2. Mohammed_Lee

    How do I prevent getteing "dust" of Molsieves in the dryed Chemicals?

    Question 
    some sources say up to 400°C, guess that also confused me. I did it now in a DIY vacuum pot, worked fine!
  3. Mohammed_Lee

    Synthesis with H2S04 and CaCO3/CaO?

    I have some pharmagrade concentrated HCl (37%) left and I'm interessted in turning some base into Amph-HCL. Is it made like Sulfate (adding HCl dripwise) or by using gaseous HCl? thx in advane
  4. Mohammed_Lee

    How do I prevent getteing "dust" of Molsieves in the dryed Chemicals?

    Question 
    Ah, I didn't see the f after the °. Perfect, thx
  5. Mohammed_Lee

    Why is there no amphetamine in the form of oxalate salt

    Hi! Do you have experiance in producing amphetamine hcl or any liks sbout its production?
  6. Mohammed_Lee

    I need help.

    Question 
    depending on your budget you can use the ventilators from grow tents to blow the gas outside. Another option would be: open the windows and don't directly inhale the fume. In my opinion and if its only a one time thing: with 150 ml of Methanol you'd really really have to be unlucky or unable to...
  7. Mohammed_Lee

    Vet or Medical ketamine

    Question 
    oh.. i misunderstood, sorry. another vendor I tried i s Ketamin spray from NL but the dosses he sells are more against depression..
  8. Mohammed_Lee

    How do I prevent getteing "dust" of Molsieves in the dryed Chemicals?

    Question 
    ok.. so I guess about 2 days with the 220 mine is capable of 😂
  9. Mohammed_Lee

    Vet or Medical ketamine

    Question 
    I got som from a german vendor called Dr. Drosden some time ago, he sold both.. But idk if he is still active.
  10. Mohammed_Lee

    HgCL2 Hydrophil?

    Question 
    Hi, I got about 5 g of HgCl2 in a small vial stored at RT. it sems to get stickier from time to time. Is It a hydrophil substance? Whats the best way to store small ammounts (I got about 80 g vacuum sealed)? thx in advance
  11. Mohammed_Lee

    Producing RM For Amphetamine Al/Hg sythesis on stock

    Question 
    Hi, since I want my Production to be a bit more efficent I got a Question: Can I mix RM for Amphetsmine via Al/Hg Synthesius on Stock (for about 10 runs). Maybe without adding the HAc? If yes: store in fridge or RT? thx in advance
  12. Mohammed_Lee

    How do I prevent getteing "dust" of Molsieves in the dryed Chemicals?

    Question 
    thx for the Answer. Since I don't own a vacuum stove. can I regenerate them in a regular one? How many °C would you recommend?
  13. Mohammed_Lee

    How do I prevent getteing "dust" of Molsieves in the dryed Chemicals?

    Question 
    Like the title says: whenever I store a Liquid over a molecular sieve the Liquid gets light brown fron the sieve. I didn't manage to filter it out with all the types of filters I have at home. Which ones are suited, is there another way? thx in advance
  14. Mohammed_Lee

    Sulphuric acid

    there are some videos on youtube describing the whole process pretty good
  15. Mohammed_Lee

    Problems with synthesis of amphetamine phosphate from P2NP via Al/Hg

    Something strange happened during Washing. I added about 4 times the Volume of Aceton and got a deep Orange upper layer. I measured pH again and it still was somewhere between 6-7 after adding a drop of 1:1 Aceton H3PO4 it went to 6. I transferred the upper layer into another beaker, added a...
  16. Mohammed_Lee

    Problems with synthesis of amphetamine phosphate from P2NP via Al/Hg

    Did you also have problems with over acidifying the base. I just evaporated the next batch and again: I stopped adding H2PO4 when I was more on the pH 7 than 6 range and the batch got pink/red after drying. Is it possible that it has something to do with the evaporation process, should I add...
  17. Mohammed_Lee

    Problems with synthesis of amphetamine phosphate from P2NP via Al/Hg

    I did so and with consultation from "the money" I came to better results. Now I'm optimizing my technique while waiting for the results of analysis. Here's a summery of my next tries: The chemicals I used: Al Foil (I don't know how many um but the premium one from Supermarket, thicker than the...
  18. Mohammed_Lee

    Problems with synthesis of amphetamine phosphate from P2NP via Al/Hg

    Update: I decided to put the middle and upper layer in a separatory funnel drained the middle layer back to the beaker and added phosphoric acid but no salt fell out (even after I added enough to reach pH 3).
  19. Mohammed_Lee

    Problems with synthesis of amphetamine phosphate from P2NP via Al/Hg

    Hello, as I already described in another thread I got problems with the synthesis of amphetamine phosphate from P2NP via Al/Hg. I already made two Batches withe the same result: a much to high yield of whatever anorganic salts (for example 85g from 10g of P2NP). I followed every step from the...
Top