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so I did. or could it be caused by too high pH of the amine .. I think it is too alkaline. you can hardly see the difference on the strips, but it seems to me that the pH is 13-14 the next time after the reaction is complete, I will want to lower the pH with acetic or hydrochloric acid and...

why the synthesized amphetamine has no power? everything done as it was written in the recipe. the smell is there, the taste is bitter, and the potency is very weak… what could it be?

one of the experts could explain this inaccuracy heh

in your opinion, after adding the base and the oil flows out, IPA is added and mixed and then the top layer is pulled off?

gentlemen, I still did not get a reply to point 7. for me, after removing the top layer and adding to the bottom (water) IPA NOTHING HAPPENS. two layers are not formed again

I wonder if it will not be better if in the end you will not add 50% acetic acid to get down from the pH lower and then add a little alkali to these 12… what do you think?

aaa and the question is what pH should be after the end of the reaction? mi shows 10-11. after adding alkali the base pops up and it is 12-13.

Ok, did I count well for 250g p2np that I would need 550g NaOh in 1650ml dh20? I found a dependence that the NaOh solution was added in the proportion of 44% to the amount of IPA + dh20

gentlemen, how do we know what volume of 25% NaOh solution should be added? I mean where did this 8 l come from, how to calculate it?

I already know that there is good in the upper part. what then in the bottom?

gentlemen, during the evaporation of IPA two layers are formed, one milky the other yellowish. freebase in the milk phase?

no separation occurs after phase separation and addition of IPA to the aqueous phase.

but this aqueous layer is formed during the reaction. to separate and for scrap?

what do you mean ?

gentlemen, reading all this and doing it myself I got confused ... namely after adding cucl2 after a while two layers are formed for me, why? I form two layers before adding the alkali. when added, the oil seemed to mix with the top layer.

after adding 25% NaOh solution, phase separation, I added 1/3 dcm of the volume of aqueous solution. my question at what temperature should I distill? in my opinion, apart from freebase, there is still water in this solution, IPA and dcm, am I right? then distillation at Ok 83 degrees?the...

Will the 500ml / min dosing peristalic pump handle the 500mm jacket length reflux condenser demand? there is a problem with access to tap water, therefore the inquiry….

this system works very well with bromination, but I do not have enough knowledge to say that it can handle it ... hence my question addressed here ...

I have one more question, will the cascade absorption consisting of a buffer and two Dreschl washers filled with a 10% alkali solution be able to eliminate the smell emitted during the reaction? everything, of course, connected to the radiator in advance. the diagram is supposed to look...

I have a question: is there a difference in power when doing it with p2np and with bmk?