Can the reduction of these nitropropenes be completed with the IPA/Water 2:1 + NaBH4 + CuSO4 methods used for amphetamines just as easily? I know LAH in thf is called for here, but lacking any formal chemistry education I don't know if there will be any interaction with the supposedly vulnerable...
Well, i did it anyway. Definitely pyrophoric... ***** lol.... But i suppose that doesnt really mean much... What makes professionally made catalysts better?
From what i gather its just find some activated fine powder carbon, heat with 10% nitric acid solution for a few hours. Rinse. Dry. Add 5 or 10% by weight palladium into a beaker, dissolve with hcl/h202. Add to beaker with activated carbon and stir for a bit to let it soak. Then add formic acid...
your clarification here across three comments here has been the most clarifying and absolutely useful thing ive *****en read in a while. thank you. I know you posted this like 8 months ago so im just saying it now in case no one else does, this is what i needed to clear the air about all this...
ive gotten that syrup a few times too.... no idea what it is either, and id get that using sulfuric acid. usually happens when i use too much and go below ph 6, but idk could be a fluke... ive failed many more times than ive succeeded, but ive succeeded, found a method that works great for me...
Yea, tell me this after i do exactly this, also i should have known tbh.
Before i did anything, I sat there for 20 minutes and thought wtf can i use as a solvent for sulfuric acid that it wont react with... idk why i didnt think of alcohol... i think i just remembered its dehydrating power and...
no hes right, its this white kind of stringy shit. doesnt seem to dissolve in water. If you leave sulfuric in acetone long enough in high concentrations it also turns red.... least it did with me...
I know concentrated sulfuric acid has no water in it so thats ideal when making a salt, but is this the main reason for seeing sulfate salts as the way to go on most tutorials?
I FINALLY *****ing suceeded in getting amphetamine freebase and now the question is, gas it or acetone/sulfuric acid...
im in the USA, are PO boxes safe enough anymore? how does this work? How do i receive this kind of stuff.... I ask because with importation from another country, the last thing i want is customs being able to track me down, worst case scenario... Or even domestically i just cant chance any...
Yea and the molar ratio of whats in the video is basically 1.5 times as much nitroethane as benzaldehyde. instead of 4.44...... same amount of liquid for each but nitroethane weighs less so youre actually adding more nitro than benzaldehyde even if youre addding the same volume of each.
i...
.060 mol benzaldehyde + .266 mol of nitroethane -> .038 mol of P2NP
68% of the benzaldehyde was made into P2NP
there is 4.4 times more nitroethane than benzaldehyde
hell of an excess for yield that's average at best.
im pretty sure if you add a solvent like glacial acetic acid, and instead of...
Sooo i finally got some sassafras oil and im seeing several ways to do this...
The most common seem to be:
the freeze crystalization of safrole
vacuum distillation
liquid/liquid extraction
( https://www.drugtimes.org/ecstasy-3/safrole.html kind of goes over a bunch of methods if anyones...
well, look at it like this. Making any drug is actually fairly easy if you have the ingredients more than anything. The correct equipment is second because if you can find the chemicals, then you can make the adderal with a few glass jars and coffee filters. If you dont have all the ingredients...
the only way you have a chance is if you can get your hands on benzaldehyde and nitroethane (in the usa forget about it unless you have connections which you probably dont if your asking for help on synthesis)..... If not, its pretty much out of the question unless you want to seriously start a...
dude.... wow... thats a damn good article.. thanks for finding that...
I have not done this yet, i did just spend the weekend making it with the sulfuric acid oxidation of BzOH in DMSO route.... via reflux... only an hours worth of refluxing but good god the DMSO thermally decomposes and you...
you need to do what is called an acid base extraction, Guy above my comment is basically giving you the basic idea. you can use more than naptha, it can be toluene, hexane, ether, whatever, anything non polar. you'll find a description of this mechanism on the 3rd page of the videos section. its...
Can copper sulfate be used instead? thats dirt cheap at the hardware store as tree stump killer... Making copper chloride isnt hard but would be annoying... same with buying it, but either way, would it work ya think?
wow finally a video that explains it. right on thanks man!
malic acid is added to D-amphetamine freebase and then is water soluble. Extracted with water, basified, extracted and reprecipitated. For some reason it was so hard to understand that before... thanks for making this