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Hello. now we managed to build a steam distillation system. with the help of a nice forum member. the distillation is currently in progress, I think I'll be done in 2 hours 😉 I'm only making a small amount now, if I succeed, I'll use 1kg p2np. I don't have the opportunity to dry it outdoors...

Is constant stirring necessary during water steam distillation? Thx ansver

7. The aqueous phase is extracted with 8 liters of IPA. Amphetamine free base is dissolved in IPA and IPA layer density is changed, hence, it is separated from aqueous layer. 8. The IPA from step 7 extract is evaporated on vacuum to an amphetamine free base oil and combined with free base from...

I want to carry out steam distillation of water in a reactor. first the IPA evaporates, then I change the collecting flask, the water and oil leave together as steam, the oil will become transparent, it will float on top of the water, I just have to separate it. Well, I will soon start my...

I messed up the kayak. I cleaned the mixture on the filter and threw away the insoluble precipitate. I poured it back into a reactor. I added a 25% NaOH solution. two layers formed. I rest for half an hour. upper yellow layer (Ipa/base). bottom layer transparent (water layer). I drop the...

I don't think you should do anything with the IPA/base after the election. there is too much alcohol in it, I would like to reduce the ipa. I think the quality of the oil may be poor due to too much IPA.

This is what Ipa/free base looks like after Ipa evaporation. it was almost 6 liters. when I started, the color was lighter and it had a pleasant smell, stronger than now. maybe i burned the base??

Ipa párolgás után így néz ki az Ipa/free base. majdnem 6 liter volt. amikor elkezdtem világosabb volt a színe és kellemes illata volt, erősebb mint most. lehet, hogy elégettem az alapot??

hello gentlemen ! The IPA from step 7 extract is evaporated on vacuum to an amphetamine free base oil and combined with free base from step 6. I evaporated it into my vacuum and this is what I got. this is good ? (first picture) what to do with this, because it doesn't smell like an amf...

I want to make bmk oil, could you help me?

Hello. 10L IPA Distilled water 3.1 L; Sodium borohydride (NaBH4) 870 g; P2NP (Phenyl-2-propanone) 500 g; Copper (II) chloride (CuCl2) 52 g. Sodium hydroxide (NaOH) water solution 25% 4 L;. these reagents . this was the bottom layer (water layer). I added Ipa these layers are...

Hello. 10L IPA Distilled water 3.1 L; Sodium borohydride (NaBH4) 870 g; P2NP (Phenyl-2-propanone) 500 g; Copper (II) chloride (CuCl2) 52 g. Sodium hydroxide (NaOH) water solution 25% 4 L; I use these reagents. I observe temperature regulation. I add it to 4L of 25% naoh reaction...

this would be the aqueous layer. I added 25% naoh solution. which layer do i need ?? I was a little confused

I use a gentle vacuum. it does not suck the alcohol towards the condenser. what evaporates flows back. maybe a stronger vacuum is needed?

managed to dose p2np . I simply poured it in several parts through an opening. I'm trying to vaporize IPA now. I'm at 80 degrees but it's not steaming. I use rotovap without vacuum. anyone have an idea?

hello gentlemen, how can I feed p2np into the reactor? there is a 2000ml dispenser but it gets clogged. need to be unlocked ?? if so, with what? as far as I know, the reactor cannot be dismantled during work.

Hello. add nabh4, I turn on the mixer. What is the recommended mixing speed (rpm)? can the speed be the same while administering nabh4, p2np, cucl2? Step 5: keep warm for 30 minutes at 80 degrees, is mixing necessary here? Thank you for your answers

I want to build a steam distillation system, I'm just stupid. I know there are many systems. I want to purify free base from water, IPA. to win oil. I want a user-friendly system for beginners. instead of an oil and water bath, a heating mantle is suitable, I know it is a more expensive...

what does a high-pressure steam cleaner look like? I want to build a steam distillation system, but unfortunately I can't order it, I don't know what I want, what the device is called.

2*5L 2 Neck RBF 2*5L magnetic stirrer heating mantle Connector joints 1*Chilling column 2* 2 way distillation connector. this information was shared with me by a dear forum friend. I don't understand what chilling column means. how many pieces and what kind of connectors do I...