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  1. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    For me the A-Oil is : Here I hate this langage. It would be easier if people talked about molecules and not about a language coming from the street...
  2. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    This is what you did for 24 hours (4x6h) and that led to your "A-Oil": "Amphetamine has been synthesised from l-phenyl-2-propanone (P2P) via N-formylamphetamine using ammonium formate. l-Phenyl-2-propanone and ammonium formate, (...) were combined and heated (160-180° C )" But your...
  3. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    "Amphetamine has been synthesised from l-phenyl-2-propanone (P2P) via N-formylamphetamine using ammonium formate. l-Phenyl-2-propanone and ammonium formate, (...) were combined and heated (160-180° C ) The contents of the distillation flask were then cooled and hydrolysed by heating with...
  4. serialz

    IM LOOKING TO BUY

    Looking for a vendor 
    Yes, without any problems. You should always read the customer feedback if you don't know the shop that sells on Alibaba. (Store score)
  5. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    Thank you, there is no obligation at all. I consider it normal to help
  6. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    An impure molecule, as the name suggests, is a molecule mixed with, for example, traces of solvent or another molecule. (Water, acid, etc) Hence the importance of separating, cleaning, distilling and drying the p2p. This will become more technical. We're talking about "mole" ratios. In this...
  7. serialz

    Need a little help with something

    Question 
    Hi, The solution is here
  8. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    Take this pdf. All the method with the formic is on this pdf page 33 and after. Don't forget that your orange oil is phenylacetone or p2p or 1-phenyl-2-propanone. This will help you find your way around the pdf. What you call A-Oil is N-Formylamphetamine. You will find everything you want in...
  9. serialz

    A-Oil to Hcl Amphetamine

    All methods to obtain A-Oil and after amphetamine
  10. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    I'll explain what you just did is called a decarboxylation. If your starting molecule is the cas 5449-12-7 and his name is BMK Glycidic Acid (sodium salt): Mechanism: BMK at the end of mechanism is Benzyl Methyl Ketone or P2P (Your orange oil) The method you want to use with formic acid is...
  11. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    If I understand correctly you got P2P (phenylacetone) You have to distil it to be as pure as possible and then you use for example this way of synthesis: Leuckart amination of 1-phenyl-2-propanone (smale scale) Or, Amphetamine from P2P (phenyl-2-propanone) And, Synthesis of methamphetamine...
  12. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    Hi, It is very interesting to vary the chemical reagents... but would it be possible to have a yield. And therefore to distil your production to have a high purity and a final product. Because without a comparison, it doesn't help much. And moreover it would be useful for the whole community...
  13. serialz

    leucart reaction

    Hi, What do you want? The reaction principle or a synthesis pathway? Leuckart reaction: (With K at LeucKart, he is a German chemist) Synthesis of MDMA from piperonylmethylketone (PMK) with Formic acid or Leuckart amination of 1-phenyl-2-propanone (smale scale)
  14. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    Use teflon, otherwise it will always be the same result. There is no such thing as good or bad stainless steel with strong acid. HCl, H2SO4, HBr, HNO3 etc. It will always be the same result. 10€ on Aliexpress...
  15. serialz

    UR-144 ingredients suppliers

    Looking for a vendor 
    Sodium hydroxide can be purchased at any hardware store. Or on the internet and totally legal as it is a toilet unblocker. For less than 10€, you can get 1kg.
  16. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    Excellent Keep us informed about the next steps
  17. serialz

    Need help convert bmk 5449-12-7 to free base A-oil

    Hello, Use a separation funnel. Keep the top part and distill only that part. Maybe you can do an additional solvent extraction for the "green" part and then evaporate the solvent and finally distill this additional part. But I'm not sure that the time versus the yield of this last extraction...
  18. serialz

    Synthesis from L-Phenylalanine to Amphetamine possible?

    Minor Strecker degradation products of phenylalanine and phenylglycine "Oxidative decarboxylation of amino acids. Amino acid (5 mmol) and potassium peroxodisulfate or glyoxal (5 mmol) were dissolved in 500 ml water and the mixture was heated in the LikensNickerson apparatus [19] for 1 h and...
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