This is what you did for 24 hours (4x6h) and that led to your "A-Oil":
"Amphetamine has been synthesised from l-phenyl-2-propanone (P2P) via
N-formylamphetamine using ammonium formate. l-Phenyl-2-propanone and
ammonium formate, (...) were combined and heated (160-180° C )"
But your...
"Amphetamine has been synthesised from l-phenyl-2-propanone (P2P) via
N-formylamphetamine using ammonium formate. l-Phenyl-2-propanone and
ammonium formate, (...) were combined and heated (160-180° C )
The contents of the distillation flask were then cooled and hydrolysed by
heating with...
An impure molecule, as the name suggests, is a molecule mixed with, for example, traces of solvent or another molecule. (Water, acid, etc) Hence the importance of separating, cleaning, distilling and drying the p2p.
This will become more technical.
We're talking about "mole" ratios.
In this...
Take this pdf. All the method with the formic is on this pdf page 33 and after.
Don't forget that your orange oil is phenylacetone or p2p or 1-phenyl-2-propanone. This will help you find your way around the pdf.
What you call A-Oil is N-Formylamphetamine. You will find everything you want in...
I'll explain what you just did is called a decarboxylation.
If your starting molecule is the cas 5449-12-7 and his name is BMK Glycidic Acid (sodium salt):
Mechanism:
BMK at the end of mechanism is Benzyl Methyl Ketone or P2P (Your orange oil)
The method you want to use with formic acid is...
If I understand correctly you got P2P (phenylacetone)
You have to distil it to be as pure as possible and then you use for example this way of synthesis:
Leuckart amination of 1-phenyl-2-propanone (smale scale)
Or,
Amphetamine from P2P (phenyl-2-propanone)
And,
Synthesis of methamphetamine...
Hi,
It is very interesting to vary the chemical reagents... but would it be possible to have a yield. And therefore to distil your production to have a high purity and a final product.
Because without a comparison, it doesn't help much. And moreover it would be useful for the whole community...
Hi,
What do you want?
The reaction principle or a synthesis pathway?
Leuckart reaction: (With K at LeucKart, he is a German chemist)
Synthesis of MDMA from piperonylmethylketone (PMK) with Formic acid
or
Leuckart amination of 1-phenyl-2-propanone (smale scale)
Use teflon, otherwise it will always be the same result.
There is no such thing as good or bad stainless steel with strong acid. HCl, H2SO4, HBr, HNO3 etc. It will always be the same result. 10€ on Aliexpress...
Sodium hydroxide can be purchased at any hardware store. Or on the internet and totally legal as it is a toilet unblocker. For less than 10€, you can get 1kg.
Hello,
Use a separation funnel. Keep the top part and distill only that part.
Maybe you can do an additional solvent extraction for the "green" part and then evaporate the solvent and finally distill this additional part. But I'm not sure that the time versus the yield of this last extraction...
Minor Strecker degradation products of phenylalanine and phenylglycine
"Oxidative decarboxylation of amino acids. Amino acid (5 mmol) and potassium peroxodisulfate or glyoxal (5 mmol) were dissolved in 500 ml water and the mixture was heated in the LikensNickerson apparatus [19] for 1 h and...