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  1. uiawghdouawhdouiawhd

    Shake and Bake Remastered

    you need isopropyl alcohol 99% if you want a high purity and big shards, or you could get 91% and dry it using anhydrous magnesium sulfate.
  2. uiawghdouawhdouiawhd

    Comment by 'uiawghdouawhdouiawhd' in media 'Amphetamine Hydrochloride Synthesis Via Phenylpropanolamine Reduction With Iodine and Hypophosphoric Acid'

    can you guys make a video on the anhydrous ammonia reduction of pseudoephedrine?
  3. uiawghdouawhdouiawhd

    Shake and Bake Remastered

    Today I will be updating my old rushed synthesis of the shake and bake. This will include proper glassware, equipment, washing of impurities, and recrystallization with additional purifications like cold anhydrous acetone washings! Precursors needed with measurements: 10 grams of ephedrine or...
  4. uiawghdouawhdouiawhd

    Shake and bake with proper equipment and techniques my way

    heres a video of the violent boiling mentioned
  5. uiawghdouawhdouiawhd

    Shake and bake with proper equipment and techniques my way

    my apologies this synthesis procedure was rushed, but if theres anything i should change about it for when i do it again like for purification etc could you explain?
  6. uiawghdouawhdouiawhd

    Shake and bake with proper equipment and techniques my way

    not sure if i can add videos but ill see
  7. uiawghdouawhdouiawhd

    Shake and bake with proper equipment and techniques my way

    my bad i didnt mean to put 75 seconds it shouldve read 120
  8. uiawghdouawhdouiawhd

    Shake and bake with proper equipment and techniques my way

    Hello i just thought i would make my own version that i have success with on here using proper equipment. i will post pictures soon. Materials used: 1000ml round bottom boiling flask ACS Grade ammonium nitrate crystals Pure Sodium hydroxide Pure extracted P-PHed or ephed Solvent containing...
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