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i have made with dcm on big scale but dcm gets to hot and it will take to much time to ad the mono40%, i did it on 60 kg 2bromo3 cloro scale. so that is why i want to choose tolueen

hello, i want to made 3cmc with the following recept but does somebody have experience with making in tolueen. 10kg 2bromo3cloro 30 L tolueen 20 L mono40% Let it stand for 5 hours, temp 60 than wash 3 times with water 5 Liter of water and 4/5 liter hcl till ph 5 separte the water layer and...