Search results

MDA Hi! One could be looking for advices for synthesizing MDA from PMK. PMK- ethyl glyc. -> PMK Q1) Could/should one vacuum distill PMK to purify? Anyone knows PMK distill temp at vacuum pump level vacuum? Then reductive amination of PMK with anhydrous ammonia and hydrogen in presence of...

Ar Are you talking about MELTING something??? Wow, I could have never figured out that if you heat a wax it actually melts and turns into an oily thing… People, please do your research, read, then come here and ask specific questions… There’s a basic chemistry knowledge required for all this...

Two more things: - How about using ammonia instead of methylamine, and ethanol instead of methanol, same procedure and quantities would apply, right? - What should be the shaker frequency?

Great post! How about using an aluminum fire extinguisher, with PtO2?

Did you try this? Can you share some results? I’m deciding which way to go, but there’s too little info… Thanks!

Visual aspect of a substance is characteristic of it, if there is a notable difference then it might mean it has high amount of contaminants. Do you vacuum distill the ketone? Or just remove the water? I’m waiting for some PMK ethyl gly…

On what proportion? Also, I’ve read that catalytic hydrogenation of nitromethane gives low yields… I’m curious about this, because I can get nitromethane, but not methylamine… so this would be excellent… Can you share some knowledge?

I have similar questions but for MDMA, were you able to work something out? You think it would be better to use adams catalyst or Pd/C? Would it work in one step for MDP2P+ nitromethane?

Surfing through Google, looking for Hive stuff

Can any other solvent be used for the extraction? What's the expected yield of the method? Dissolving in boiling methanol and quenching in cold acetone doesnt seem very practical from my perspective, because acetone is strictly regulated here. Could it be dissolved in IPA/HCl and cristallized in...