Hi, I have a few questions about this route.
Methylamine 40% solution is in water or methanol ?
Can benzene be replaced with hexane or DCM or another solvent?
For scale this down like on the range of 10g 4-mpf. Is correct to scale down all the others reagents in the same 10/1 way?
Thanks
Hi,
I was looking for DCM on painting stores. It is used for removing paint. I read the formula of one of them. it is 74.5 % DCM, 1.79 % toluene, 11.6 % 1-butanol and 5.13 % ammonia.
Is there a way to purify the DCM from all that mixture? Can I carefully distillate it ?
Thanks!
Hi!
Can I replace NMP with DMSO (Dimethyl sulfoxide)?
If so, what amound I would need?
Also apart of benzene, toluene, xylene, DCM, ethyl acetato, what else can I use?
Thanks
Hi!
Is there any improved 2c-e synthesis method to produce it on large scale?
Is it possible to do it with regents that can be found on china suppliers?
Thanks!
HI, Thanks for sharing this synthesis, I think is very clear.
I am from South America and here is a little difficult to find DCM. However, I can try to find it in some way. Maybe buying it from china.
I want to ask. Can you put all the regents in a list with quantities to make a little more easy...