What defat? There's no fat, as it's not a plant extraction. Or you doing the reaction in a dirty saucepan with some cooking oil left?
You say it's getting red, that's normal if you leave it in open air.
You extract with DCM then evap the DCM as much as possible. Then add to that same flask...
My man don't do that, just take harmalas or some other maoi and eat if you want a slower onset, more mellow trip. Or eat harmalas and then take small tokes of dmt dissolved in vaping liquid straight out of a vape.
It doesn't get too warm with addition of the formaldehyde. The error is earlier, it's just that you didn't start cool enough. Then also assure you have a very good mixing and add borohydride so that you add in powder of the borohydride and not big clumps/rocks of it. Put it on paper on something...
Yellow-orange-reddish oil is good. Yes this shit is hard to disolve, use more heptane and then cool it down, no need to evap.
No problem with adding all the formaldehyde at once. Just do it again, extract immediately using more heptane and you are good I think.
No, I haven't tried the STAB route, as supposedly it doesn't work with mexamine.
Some people have preffered cyanoborohydride like this guy: https://www.thevespiary.org/talk/index.php?topic=15189
Here's the best DMT thread at The Vespiary...
"Mr. Reddit", is she, Norolinda. Just do it exactly as she did and you will succeed. Maybe you can wait shorter between addition, repeat immediately when when the temperature drops enough. I don't know how low is enough. 0C or slightly below should be ok, you can try -5C or -10C and report your...
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