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i've got no cycclohex , ive got n-butlyamine , always confused what part to use, i wrote to ghost and other no reply

My guess from the picture is the clear solution is unreacted benzo and GAA. heat it to evaporate out the GAA and then add IPa and freeze it overnight, we will see tomm what happens

ammonium acetate :D output is so racemic

Update it, I'm curious

10ml nitro and 10ml benzo .. how much GAA and how much n-butlyamaine you would use in this case ? how's the yeild btw in the equi volume ?

you may uses n-butlyamine if you are aisan

youre right its a equimolar ratio of both but considering densities of benzaldehyde and nitroethane calculate the values of both appropriately

how did you come up with those ratios ? those dont sound so stoichiometric to me.

sorry im a noob here trying to undestand, what do you mean yeild is 60-70% ? is it 60% of 10g of p2np that is 6 grms or (12al+10p2p=22grm) 60% of 22 grms = 13.2 grams ?

follow this process to end up with crap

is it 55grams benzaldehyde or 55ml ? coz density is 1.04gm/L and in the picture your flask size is 200ml , so im guessing it must be 55ml please suggest

with same quantities can you suggest what quantity of n-butlyamine to be used ? instead of cyclohexylamine ?

Found this in Rhodium : Written by Zorohustra Chemicals 80 mL Toluene (ACS) 40 mL Benzaldehyde (~99%) 30 mL Nitroethane (>99%) 10 mL n-Butylamine (p.a.) Do we need to use toluene aswell ? can someone post measurments for small scale.. iam trying to get 10grams P2NP

good question.

this is no meth , can you write from here on how to make it to crystal meth

THAT went over my head. i have amp salts now how do i convert to meth crystals ?

can we linear scale down this ?

Hi , please can anyone provide small scale, synthesis procedure for this , i have 100grms of p2np

THAT'S THE FINAL PRODUCT OR THERE IS MORE TO IT ? WHAT ABOUT CRYSTALLIZATION ?

are you sure its cyclohexylamine ?