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    GBL synthesis

    Have you got a link to find this cleaner in china. I’ve searched everywhere for something like this and found nothing.
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    Methamphetamine synthesis from P2P via Aluminum amalgam

    With the amalgamation is there a reason why it goes for 15min? Cause I think I used to much mercury 2 nitrate and had to stop it within 5min is that a problem?
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    1-Phenyl-2-propanone (P2P) Leuckart amination to amphetamine and methamphetamine. Smale scale.

    Do you mind giving me a little more info on prevent alkaline hydrolysis. As I’ve done the reaction and now have produced as a dark oil in toluene. can I just steam distill by adding water to Rm or better to add aq Noah solution?
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    P2P synthesis from BMK glycidate ethers

    Yeah I got Fuk all from first attempt, will try again with phosphoric acid.
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    P2P synthesis from BMK glycidate ethers

    In reagents it’s 80ml hcl but step 2 it’s 200ml hcl?
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    P2P synthesis from BMK glycidate ethers

    I’m about to start first attempt so any other tips or tricks I should know I’m all ears.
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    P2P synthesis from BMK glycidate ethers

    Sorry I got another dumb question! When skip step 1 and start at acid hydrolysis cause have the sodium salt, Do I start by adding the Bmk then start with small portions of acid 200ml? Just not sure if I should be dissolving the salt in water before start with acid or acid straight onto salt?
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    P2P synthesis from BMK glycidate ethers

    I got BMK powder but not sure if sodium salt, how to tell the difference between each?
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    1-Phenyl-2-propanone (P2P) Leuckart amination to amphetamine and methamphetamine. Smale scale.

    7. Crude methamphetamine free base is distilled under vacuum (2 mbar, 60-100 °C) with help of Kugelrohr distillation apparatus (optional) to yield methamphetamine as a clear to pale yellow oil (2.5 g, 42%). What’s other option? Simple, fractional or steam distillation? If don’t have Kugelrohr...
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    Phenyl-2-Nitropropene synth help

    Thanks mate, much appreciated
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    Phenyl-2-Nitropropene synth help

    Sorry if this is common knowledge but I’m ready to attempt the p2np synth from Benzaldehyde, Nitroethane and methylamine. It ask for 15 mL dilute aqueous methylamine in 150 mL alcohol. how do I convert methylamine HCl to this and how many grams to make the 15ml aqueous solution. any help would...
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    How to Extract THF From PVC Glue?

    I’m wanting to do this as well, any help would be much appreciated.
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