With the amalgamation is there a reason why it goes for 15min? Cause I think I used to much mercury 2 nitrate and had to stop it within 5min is that a problem?
Do you mind giving me a little more info on prevent alkaline hydrolysis.
As I’ve done the reaction and now have produced as a dark oil in toluene.
can I just steam distill by adding water to Rm or better to add aq Noah solution?
Sorry I got another dumb question!
When skip step 1 and start at acid hydrolysis cause have the sodium salt,
Do I start by adding the Bmk then start with small portions of acid 200ml?
Just not sure if I should be dissolving the salt in water before start with acid or acid straight onto salt?
7. Crude methamphetamine free base is distilled under vacuum (2 mbar, 60-100 °C) with help of Kugelrohr distillation apparatus (optional) to yield methamphetamine as a clear to pale yellow oil (2.5 g, 42%).
What’s other option? Simple, fractional or steam distillation? If don’t have Kugelrohr...
Sorry if this is common knowledge but
I’m ready to attempt the p2np synth from Benzaldehyde, Nitroethane and methylamine. It ask for 15 mL dilute aqueous methylamine in 150 mL alcohol.
how do I convert methylamine HCl to this and how many grams to make the 15ml aqueous solution.
any help would...