Today I will be updating my old rushed synthesis of the shake and bake. This will include proper glassware, equipment, washing of impurities, and recrystallization with additional purifications like cold anhydrous acetone washings!
Precursors needed with measurements:
10 grams of ephedrine or...
my apologies this synthesis procedure was rushed, but if theres anything i should change about it for when i do it again like for purification etc could you explain?
Hello i just thought i would make my own version that i have success with on here using proper equipment. i will post pictures soon.
Materials used:
1000ml round bottom boiling flask
ACS Grade ammonium nitrate crystals
Pure Sodium hydroxide
Pure extracted P-PHed or ephed
Solvent containing...