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  1. Sitr1x

    Comment by 'Sitr1x' in media '2-Iodo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone'

    Could anyone do a video or provide some instructions on making general 4-methylpropiophenone please. This is where I'm stuck. Would be much appreciated :)
  2. Sitr1x

    Synthesis of 4-methylpropiophenone from 4-methylbenzaldehyde with diazoalkanes

    Thanks G and serialz for replying. Lol, yes the word "recipe" is very strange when you use it in such context as Chemistry, sounds like your cooking up some big dinner 🥣 Plan on using a gas trap for sure when I get to that part. Am going to try to nail the 2-iodo-methylpropiophenone bit first...
  3. Sitr1x

    A start.. But still in need of some help

    Looking for a vendor 
    Thanks for your reply G. I'm certainly interested in making 4-mmc but I want to make the 4-methylpropiophenone myself instead of buying it online. I have a question on this precursor also, is 2-iodo-4-methylpropiophenone basically the same as 2-bromo-4-methylpropiophenone and can either be...
  4. Sitr1x

    A start.. But still in need of some help

    Looking for a vendor 
    Anyone? Really wanting to learn to make something useful that's not too complex or something that I can make some form of profit from.
  5. Sitr1x

    Synthesis of 4-methylpropiophenone from 4-methylbenzaldehyde with diazoalkanes

    Would this be a viable route for a new chemist to try does anyone know? https://chemistry.mdma.ch/hiveboard/novel/000423945.html
  6. Sitr1x

    Synthesis of 4-methylpropiophenone from 4-methylbenzaldehyde with diazoalkanes

    I'm really hoping there is a safer method that is "known and tested" that I can try to get some 4-Methylpropiophenone...
  7. Sitr1x

    A start.. But still in need of some help

    Looking for a vendor 
    So I've bought a full distillation kit and now have all the main equipment needed to start experimenting, but I'm still stuck on where to start things. Should I try P2NP---->P2P------>Meth? Or should I try to synthesise something like Mephedrone first? Could anyone provide me with a solid...
  8. Sitr1x

    1-Phenyl-2-nitropropene (P2NP) Video Synthesis From Benzaldehyde and Nitroethane. Henry Reaction.

    Just wondering could this method be scaled down in half of the original amounts along with a 5litre flask used for example ? Ta
  9. Sitr1x

    1-Phenyl-2-nitropropene (P2NP) Video Synthesis From Benzaldehyde and Nitroethane. Henry Reaction.

    That's a shame =( Might have to order some soon to do a test run using this method to see if it is legit ETNO2. I did read one post of someone claiming they have used it with no issue to produce P2NP so who knows. Wish I had an easy way of making it myself
  10. Sitr1x

    4-MMC (mephedrone) synthesis. Complete video tutorial.

    As I was too busy reading, I didn't realize that the Methylamine synthesis video which I downloaded in the background that I mentioned in my earlier post is actually done on a decent starting scale lol So please disregard that part. Am just going to have to wait until I get my proper glassware...
  11. Sitr1x

    1-Phenyl-2-nitropropene (P2NP) Video Synthesis From Benzaldehyde and Nitroethane. Henry Reaction.

    Just a heads up SWIM found out on the clearweb somewhere that particular 'paint brush saver' liquids contain primarily Nitroethane and isn't too much on the expensive side of things.
  12. Sitr1x

    4-MMC (mephedrone) synthesis. Complete video tutorial.

    This was my initial thought as well as I've read similar problems with other synth's on threads in the past. So I assume that one would need to synthesize the acetone themselves or can you still get away with using acetone from the store? Or is there a specific purity I should look for when it...
  13. Sitr1x

    4-MMC (mephedrone) synthesis. Complete video tutorial.

    Hey there, first time poster long time reader of the forums here and many other chemistry groups. Firstly, much respect to the Experts here for helping out a community of aspiring chemists, you have given me faith and much more hope on my journey of learning, and once I have gained more...
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