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Thank you. I think this is why my yield was destroyed the first run. I left the p2p as is and was very acidic.

How do you wash the acid out?

You mean you must hcl gas the methylketimine before the rearrangement to have decent yields?

Is it true using the freebase 2-hydroxy-2-(2-chlorophenyl)-1-cyclohexane-N-methylimine instead of hcl produces more tar? After producing ketamine oil what method works best to obtain hcl and recrystalize?

Is d-meth not d-meth? You've synthesized multiple routes and tried them?

Sell more weed. You sell 40g a week many people smoke that much themselves.

I tried both hcl and phosphoric. Then nabh4 reduction both times. I'll dm you photos if I can find it

Okay I'm going to try again. First time I got a nice smelling yellow oil but after further processing got no finished product back. I think that my oil wasn't fully converted.

Do you need to adjust the ph before further processing?

Do you have to adjust ph of p2p after conversion or you can use it as is?

Yes you can but you will have to evaporate a lot of water after to get it to crystallize. Also titration is tedious.

How to safely scale this up?

Sounds like gold yields to me. Do you use a catalyst in your lecukarts?

Okay thanks sounds like powder is the way to go. I have a sample amount of powder the conversion method is identical to wax?

Wax was the brown one. Old stock. New yellow one is much cleaner I hear. Haven't had the chance to run this yet.

You do a second acid base to remove the black substance? When I gas the freebase crystals are snow white but turn dark and contain that sticky substance after recrystalization to large shards. The dirty acetone used to wash also contains a lot of this and mdma. I've thought of trying to distill...

Very nice work. What process do you use to remove the black tar like impurity? Even on snow white crystals it appears on subsequent recrystalizations and the end product becomes quite dark.

Thanks. I have HCl on hand.

Followed it exactly. I'm thinking maybe the methylamine escaped as a gas instead of being captured by the methanol

MDMA can be done wet. But yes set temp to -10 when you add the methylamine HCl.