Hello master, if you (you) tried the shake and cook method and were successful, can you help me with this? I have never tried it and I want to learn from someone who has succeeded before. (People who have never tried it before copy and paste the forms) There is information pollution. Thank you.
You should reduce the pH to 3 with the distilled water you use as a solvent, then I increased it to p13 with Naoh solution and added dmc and separated it. dmc is ph5-6 again, then I dried the water in it and evaporated it (it is said that toulene is more effective instead of dmc but I haven't...