Convert bmk glycidiate 20320-59-6 to oil need help guys step by step if possible please

[Castlebar]

Need help and step by step instructions to convert bmk glycidiate powder 20320-59-6 to oil any information appreciated thanks

 

[G.Patton]

Hello, cas 20320-59-6 isn't BMK gycidate, It is Diethyl(phenylacetyl)malonate. 1-Phenyl-2-propanone (P2P) from Diethyl(phenylacetyl)malonate

 

[Castlebar]

Thanks Patton for reply any information on how to convert from powder form to oil would greatly be appreciated

 

[Castlebar]

Hello just too update the cas number on the bmk powder was wrong the correct cas 5449-12-7 bmk powder any information or instructions for conversion to oil greatly appreciated

 

[blackburn]

Bmk 5445-12-7 1kg
H2O 0,5 L
Phosphoric acid 85% 1,2 L


1.
Dissolve The powder in stirring with the hot H2O 0,5L

2.
Add Phosphoric acid 1,2L and reflux for 3-4h in 120c

After reflux let sit for 1 hour to cool down, then collect the too layer.

 

[blackburn]

5449-12-7*

 

[Castlebar]

Thankyou sweswe

 

[G.Patton]

There are several topics with manual. Look at Amphetamines (phenylethylamines), there is P2P synthesis from BMK glycidate ethers

 

[Castlebar]

Thanks I will look

 

[Castlebar]

Hi guys just to give you an update after taking all your advice have now managed to produce a very dark bmk oil I need to convert this from p2p to pn2p so I can make Anphetamine sulphate

 

[melk]

Don't believe everyone because it is really crazy, the amount of wrong info for this cas 5445-12-7

you need to take pictures what you do.

the info in the other topic is much better .

I am also waiting for an angel there.

 

[Castlebar]

Thanks all advice is welcome just waiting on some equipment I've ordered and chems to convert then I will do leuchart reaction and distillation

 

[KokosDreams]

I think in your situation it would also be helpful to open up a private chat.

Actually the experts here on the forum offer private consulting in private chats.

This was a big help to me in planing the lab I'll set up and also within the synthesis that I will start soon

 

[Castlebar]

THanks bro I think that could defo be the way forward I'm doing a Lil video of me making up some sulphate when I finished would like to put up if possible what you think?

 

[Castlebar]

THanks bro I think that could defo be the way forward I'm doing a Lil video of me making up some sulphate when I finished would like to put up if possible what you think?

 

[KokosDreams]

You're very welcome!

Yeah man I'd love to see it I would love if you'd post it in our group too!

I'll make sure I'll update the group with pictures and videos as much as I can in 2-3 weeks from now when I will be ready to start my adventure